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              微量水分測定儀使用說明書

              文章出處:未知人氣: 85 發布時間:2019-03-04 11:24

                微量水分測定儀使用說明書,全面詳細介紹了儀器使用、裝配、維護過程和步驟,但為了客戶能夠快速方便使用,特將儀器調試、新電解液平衡點調整的步驟簡單介紹如下,有需要的用戶快來看一下吧。

              微量水分測定儀使用說明書

                1、開箱后,要檢查配件是否齊全;

                2、將電解池從鈣塑盒中小心取出,將2支電極、干燥管(嵌入在鈣塑盒中)、進樣旋塞、電解池瓶塞取出,在所有磨口處涂很少的真空脂或凡士林待用;

                3、進樣旋塞中間硅橡膠墊已經裝好,第一次扎入進樣針時很難扎入,可用硬針頭先反復扎幾次,也可將進樣旋塞的旋塞柱松一下;

                4、將微量水分測定儀的電解液倒入池瓶下刻度線以上,再將電解液倒入電解電極(帶網子的)中約2cm高,兩液面高度目測平行即可,將攪拌子放入電解池液中。為了電解液便于保存,新鮮電解液顯棕黑色,顏色越深電解液越新鮮;

                5、將測量電極(帶2個小鉑金柱頭的細電極)、干燥管、瓶塞、進樣旋塞放置在池瓶的相應位置,將裝好的電解池放置在主機上,整個操作過程杜絕和水接觸;

                6、電解電極(帶網子的)插頭插到主機的電解插座上,測量電極插頭插到主機測量插座上,電解池放正后剛好左邊插左邊、右邊插右邊;

                7、微量水分測定儀的主機攪拌速度出廠前已調好,如需調整可在“設置界面”設定,使液面有很小的旋渦狀即可,不能速度過快,過快攪拌子跳動會打壞電極;

                8、用50μl進樣器,抽10μl水從進樣旋塞口扎入,將針頭扎到液面下,第1次可能很緊,可用手托一下,不能讓針頭彎曲。這樣反復幾次用50μl進樣器,抽10μl水從進樣旋塞口扎入,將水注入到電解液中。每進一次間隔10秒鐘,觀察顏色變化,待顏色變成棕紅色時,進樣量減為1μl水。同樣每進一次間隔10秒鐘,觀察顏色變化,待顏色變成淺黃色時開始記數,停止進水,記數至終點微量水分測定儀報警,此時電解液即為新平衡點;

                9、在正常測定樣品前,為了確定儀器、電解池、電解液整個系統的正常和準確,可用0.5μl進樣器進純水進行標定,用0.5μl進樣器進0.1μl水,顯示應在90—110μg之間,說明儀器正常,可以正常使用。

                微量水分測定儀的調試步驟一般就是這些,只有做好調試工作,才能在使用時更好的使用設備。以提高設備的工作效率和使用壽命。

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