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              卡爾費休水分測試儀的注意點有哪些?

              文章出處:艾科瑞德網絡部人氣: 102 發布時間:2018-05-17 10:04

                   
                 1、系統密度性。卡爾費休水分測試儀電解池瓶和電極、干燥管、進樣塞、液路連接等各部分之間一定要緊固。如果不密閉,會導致空氣中的水分與試劑反應,從而是滴定終點延遲,影響測試結果。

                 2、磁力棒攪拌速度。卡爾費休水分測試儀磁力棒的初始速度應調到中間位置,開始攪拌后根據液面進行調節,使攪拌速度達到最快但液面不形成漩渦即可,這樣可以最快達到滴定終點。

                 3、取樣的準確性。卡爾費休水分測試儀標定時比如取10mg水,盡量使用10ul進樣器,且要排除氣泡,確保是10ul的水,這樣才能保證標定結果的準確。測試的時候取樣也是同理,進樣前稱量一下進樣器和樣品的總重量,進樣后再稱量一下此時進樣器的重量,相減之后就可以得出進樣的樣品重量。

                 4、甲醇清洗。卡爾費休水分測試儀測試完畢后,如要清洗,需先將卡爾費休試劑排出,然后用甲醇清洗干凈即可。不可用水清洗,否則會影響下次測試時儀器的標定。  
                
                 5、遠離磁場。卡爾費休水分儀在測試時,需要遠離強磁場,避免出現攪拌異常和電子顯示跳動。

               

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